Mass Transfer Effects on Kinetics of Dibromoethane Reduction by Zero-Valent Iron in Packed-Bed Reactors

Abstract

'Mass transfer effects on the kinetics of 1,2-dibromoethane (EDB) reduction by zero-valent iron (ZVI) in batch reactors, a laboratory scale packed-bed reactor, and a pilot scale packed-bed reactor are described. EDB was debrominated by ZVI to ethylene and bromide. EDB sorption to the cast iron surface was nonlinear and was described by a Langmuir equation. Laboratory scale column studies showed a nonlinear dependence of EDB removal on flow rate and initial EDB concentration. A nonequilibrium model of EDB sorption and reaction dependent on mass transfer was constructed using the laboratory scale data. The model was verified using data from a larger pilot scale packed-bed reactor that was used to remove EDB from contaminated groundwater. The data show two distinct removal processes, an initial rapid phase dominated by mass transfer followed by a slower phase where surface reactions dominated. The model successfully predicted the transition from mass transfer controlled surface reaction controlled conditions in the pilot scale data'.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 21, 2002
Accession Number
ADA405434

Entities

People

  • David Burris
  • Gregory Loraine
  • John Schoolfield
  • Lixiong Li

Organizations

  • Applied Research Associates (United States)

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force Research Laboratories
  • Alkenes
  • Chemical Synthesis
  • Chemistry
  • Detectors
  • Engineering
  • Environmental Engineering
  • Equations
  • Ethylenes
  • Flow Rate
  • Groundwater
  • Liquid Chromatography
  • Mass Transfer
  • Organic Compounds
  • Sorption
  • Steady State
  • Surface Reactions

Fields of Study

  • Chemistry
  • Environmental science

Readers

  • Agricultural Chemistry/Soil Science
  • Combustion science or combustion engineering.
  • Nuclear Civil Defense.