SEEDLING Proposal to Establish Pilot Data for a Consortium on Magnetic Nanoparticle Assemblies: A New Tool for Drug Delivery, Sensors and Electronic Devices

Abstract

Complexes of magnetic nanoparticles with polymer dispersion stabilizers can lead to well-defined magnetic dispersions and also to precursors for magnetic microspheres. Thus, complexes of block copolymers containing both hydrophilic and hydrophobic dispersion components with magnetite nanoparticles have been prepared and characterized. In-vitro cell survival assays of the hydrophilic complexes suggest a relationship between cell survival and proliferation and the molecular weight (and hydrophilicity) of the polymer dispersants (higher molecular weight results in better cell proliferation/survival). Magnetic transition metals such as cobalt, iron or nickel are susceptible to oxidation with concurrent loss in magnetic response unless the nanoparticle surfaces are protected with oxygen impermeable coatings. Copolymer precursors to graphitic-like and silica-like protective coatings have been prepared and utilized to coat cobalt nanoparticles in thermolysis reactions. High temperature pyrolyses of the complexes in both cases suggest that oxidatively stable cobalt nanoparticles approximately 10 nm in diameter can be formed. The pyrolysis procedure results in 10-nm cobalt but the particles are adhered together. Attention will be devoted during the forthcoming year on methods for separating the nanoparticles from each other and on 're-coating' the materials with appropriate biospecific functional groups.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 01, 2003
Accession Number
ADA418026

Entities

People

  • Judy S Riffle

Organizations

  • Virginia Tech

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Sensors

DTIC Thesaurus Topics

  • Alkenes
  • Biomedical And Dental Materials
  • Block Copolymers
  • Carbonyl Complexes
  • Cell Physiological Processes
  • Chemical Synthesis
  • Chemistry
  • Copolymers
  • Heat Treatment
  • Magnetic Nanoparticles
  • Magnetic Properties
  • Materials
  • Materials Science
  • Metallic Nanoparticles
  • Nanoparticles
  • Particles
  • Polymers

Readers

  • Nanocomposite Materials Science
  • Organic Chemistry
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Biotechnology
  • Microelectronics