Freeze-Spray Deposition of Layered Alumina/Zirconia Composites (Preprint)

Abstract

A novel freeze-Spray Deposition (FSD) method is described for rapid fabrication of layered composites with controlled layer thickness and uniform microstructure. The graded alumina/zirconia composites are fabricated by freeze-spray deposition of ceramic slurries followed by freeze drying. Aqueous slurries with glycerol addition are sprayed on a cooled substrate using an automated 3-D gantry system. Processing parameters such as viscosity of the ceramic slurries, composition and thickness of deposited layers as well as sintering conditions are investigated to improve the fabrication process. Microstructural analysis of the fabricated composites revealed uniform and crack-free transitional layers indicating a strong interfacial bonding between the layers.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 2009
Accession Number
ADA503055

Entities

People

  • Ashlee Abbott
  • Fatih Dogan
  • Oratai Jongprateep
  • Qiang Fu

Tags

Communities of Interest

  • Space

DTIC Thesaurus Topics

  • Air Force
  • Air Force Research Laboratories
  • Composite Materials
  • Electron Microscopy
  • Fabrication
  • Glycerols
  • Laminates
  • Materials
  • Materials Processing
  • Materials Science
  • Microstructure
  • Physical Properties
  • Spray Forming
  • Thermal Expansion
  • Thickness
  • Three Dimensional
  • Viscosity

Fields of Study

  • Materials science

Readers

  • Nanoscale Plasmonic Nanotechnology
  • Structural Health Monitoring of Composite Structures.
  • Surface Engineering/Surface Coating Technology.