3D-Quantitative Phase Analysis and Strain Mapping of Nanostructured Coatings by Synchrotron Energy Dispersive X-ray Diffraction: A New Approach to Materials Characterization

Abstract

INTRODUCTION: Thermal Spray Coating: Fundamental Considerations * Rutgers-NSMG EDXRD Set-up at NSLS X17-B1 * Comparison of Diffraction Geometries * Evolution of Nanostructured Materials Analysis by EDXRD * Simultaneous 3D Strain and Phase Mapping in TiO2 Thermal Spray Coatings * 3D Phase Mapping of TiO2 Coating * EDXRD Quantitative Phase Analysis Results: Lattice Parameters and Cell Volume of Rutile and Anatase in Precursor Powder and TSC * Comparison with X-ray Absorption Data * Variation of strain in the coating with depth * 3D Phase Mapping in Thermal Spray coatings "Interfacial Phenomena" * Simultaneous 3D Strain and Phase Mapping in(Semi)-Amorphous Fe Thermal Spray Coatings by Combined Bragg-Brentano and EDXRD.

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Document Details

Document Type
Technical Report
Publication Date
Jun 12, 2009
Accession Number
ADA527113

Entities

People

  • A. Ignatov
  • E. K. Akdogan
  • L. Balarinni
  • M. Croft
  • M. Mcneley
  • N. Ahmedi
  • T. Tsakalakos
  • Zhaohui Zhong

Organizations

  • Rutgers University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Absorption
  • Coatings
  • Crystal Structure
  • Diffraction
  • Energy
  • Geometry
  • Materials
  • Materials Science
  • Mechanical Properties
  • Phase
  • Radiation
  • Substrates
  • Synchrotrons
  • Thickness
  • Transitions
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Materials science
  • Physics

Readers

  • Pulsed Power and Plasma Physics.
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Microelectronics