Sulfur-Doped Zinc Oxide (ZnO) Nanostars: Synthesis and Simulation of Growth Mechanism

Abstract

We present a bottom-up synthesis, spectroscopic characterization, and ab initio simulations of star-shaped hexagonal zinc oxide (ZnO) nanowires. The ZnO nanostructures were synthesized by a low-temperature hydrothermal growth method. The cross-section of the ZnO nanowires transformed from a hexagon to a hexagram when sulfur dopants from thiourea [SC(NH2)2] were added into the growth solution, but no transformation occurred when urea (OC(NH2)2) was added. Comparison of the X-ray photoemission and photoluminescence spectra of undoped and sulfur-doped ZnO confirmed that sulfur is responsible for the novel morphology. Large-scale theoretical calculations were conducted to understand the role of sulfur doping in the growth process. The ab initio simulations demonstrated that the addition of sulfur causes a local change in charge distribution that is stronger at the vertices than at the edges, leading to the observed transformation from hexagon to hexagram nanostructures.

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Document Details

Document Type
Technical Report
Publication Date
Oct 01, 2011
Accession Number
ADA552483

Entities

People

  • Erica Lin
  • Henry O. Everitt
  • Jay G. Simmons Jr.
  • Jianqiu Yang
  • Jie Liu
  • Jinhyun Cho
  • John V. Foreman
  • Jungsang Kim
  • Qiubao Lin
  • Sungwoo Yang
  • Weitao Yang
  • Yingwen Cheng

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Abstracts
  • Aqueous Solutions
  • Band Gaps
  • Charge Density
  • Chemical Vapor Deposition
  • Chemistry
  • Electron Microscopy
  • Emission
  • Energy
  • Energy Bands
  • Materials
  • Nanostructures
  • Nanowires
  • Optical Properties
  • Simulations
  • Spectra
  • Spectroscopy

Fields of Study

  • Materials science

Readers

  • Graph Algorithms and Convex Optimization.
  • Materials Science and Engineering.
  • Organic Chemistry

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene